Kinetics of the Synthesis of Aluminum Boride by the Self-Propagating High-Temperature Synthesis Method
نویسندگان
چکیده
The influence of certain factors on the kinetics process obtaining aluminum borides (burning rate, ingot formation, and phase separation) was investigated. In this study, we report registration diboride using SHS protocol. synthesis from boric anhydride occurred by aluminothermic method. initial components were boron trioxide in form powders. Researchers paid special attention to degree grinding charge fluxing substances. had rate development concentration studied. To calculate charge, a composition chosen according speed obtained number experiments where melting carried out with following densities g/cm3: 0.80; 1.08; 1.18; 1.74. method ignition above. experimental results allowed us conclude that nature change combustion system, there an excess reducing agent is same. An increase up 20%, likely due fact reaction area increased. addition, can be explained decrease heat losses reduction time. With above 20% stoichiometry, observed specific aluminum, which played role ballast.
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ژورنال
عنوان ژورنال: Ceramics
سال: 2022
ISSN: ['2571-6131']
DOI: https://doi.org/10.3390/ceramics5030033